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Anomalies in Young's modulus behavior after annealing in polycrystalline SmS

V. V. Kaminskii1, , N. V. Sharenkova2, G. A. Kamenskaya2, M. A. Grevtsev2 and Yu. V. Lyubimova1

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 Corresponding author: V. V. Kaminskii, vvkaminskii@itmo.ru

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Abstract: In this paper, the dependencies of Young's modulus and attenuation decrement on samarium sulfide polycrystals (SmS) under various annealing temperatures are studied by the piezoelectric ultrasonic composite oscillator technique at a frequency of 100 kHz in the temperature range of 80–300 K. A decrease in Young's modulus with an increase of the annealing temperature due to the texturing of the material was revealed. At the same time, attenuation peaks were observed at temperatures about 90 and 125 K, presumably due to Niblett-Wilks and Bordoni relaxations.

Key words: SmSultrasonic spectroscopyYoung's modulusannealing in polycrystalsBordoni relaxationsattenuation decrement



[1]
Takenaka K, Asai D, Kaizu R, et al. Giant isotropic negative thermal expansion in Y-doped samarium monosulfides by intra-atomic charge transfer. Sci Rep, 2019, 9, 122 doi: 10.1038/s41598-018-36568-w
[2]
Kaminsky V V, Soloviev S M, Khavrov G D, et al. Mechanism of the semiconductor –metal phase transition in Sm 1 – xGdxS thin films. Semiconductors, 2018, 52(1), 41 doi: 10.1134/S1063782618010116
[3]
Sharenkova N V, Kaminskii V V, Golubkov A V, et al. The structure of a metallic-phase film produced by mechanical polishing of polycrystalline SmS. Phys Solid State, 2005, 47, 622 doi: 10.1134/1.1913970
[4]
Kaminskii V V, Lanyi S. Semiconductor–metal phase transition under a strain induced by a spherical indenter. Tech Phys, 1998, 43, 314 doi: 10.1134/1.1258916
[5]
Sousanis A, Smet P F, Poelman D. Samarium monosulfide (SmS): reviewing properties and applications. Materials, 2017, 10, 953 doi: 10.3390/ma10080953
[6]
Kaminskiĭ V V, Didik V A, Kazanin M M, et al. Thermovoltaic effect in polycrystalline samarium sulfide. Tech Phys Lett, 2009, 35, 981 doi: 10.1134/S1063785009110030
[7]
Kaminskii V V, Solov’ev S M, Khavrov G D, et al. Structural features of Sm1 – xEuxS thin polycrystalline films. Semiconductors, 2017, 51(6), 828 doi: 10.1134/S1063782617060124
[8]
Pronin I A, Averin I A, Bozhinov A S, et al. The thermovoltaic effect in zinc oxide inhomogeneously doped with mixed-valence impurities. Tech Phys Lett, 2015, 41, 930 doi: 10.1134/S1063785015100132
[9]
Kaminsky V V, Molodykh A A, Stepanov N N, et al. The application peculiarities of semi-conducting resistive-strain sensors and baroresistors on the basis of samarium sulphide. Nauchnoe Priborostroenie (Scientific Instrumentation), 2011, 2, 53
[10]
Kustov S, Golyabdin S, Ichino A, et al. A new design of automated piezoelectric composite oscillator technique. Mater Sci Eng A, 2006, 442(1), 532 doi: 10.1016/j.msea.2006.02.230
[11]
Robinson W H, Edgar A. The piezoelectric method of determining mechanical damping at frequencies of 30 to 200 kHz. IEEE Trans Sonics Ultrason, 1974, 21(2), 98 doi: 10.1109/T-SU.1974.29798
[12]
Pal’-Val’ P P, Pal’-Val’ L N. Low-temperature internal friction and nanostructured metal stability. Met Sci Heat Treat, 2012, 54, 234 doi: 10.1007/s11041-012-9488-1
[13]
Lin D, Xu L, Jing H, et al. Effects of annealing on the structure and mechanical properties of FeCoCrNi high-entropy alloy fabricated via selective laser melting. Addit Manufact, 2020, 32, 101058 doi: 10.1016/j.addma.2020.101058
[14]
Wang Z, Baker I. Effects of annealing and thermo-mechanical treatment on the microstructures and mechanical properties of a carbon-doped FeNiMnAl multi-component alloy. Mater Sci Eng A, 2017, 693, 101 doi: 10.1016/j.msea.2017.03.099
[15]
Pal-Val P P, Loginov Yu N, Demakov S L, et al. Unusual Young׳s modulus behavior in ultrafine-grained and microcrystalline copper wires caused by texture changes during processing and annealing. Mater Sci Eng A, 2014, 618, 9 doi: 10.1016/j.msea.2014.08.069
[16]
Scharer U, Wachter P. Brillouin spectroscopy on doped SmS. Physica B, 1997, 721, 230 doi: 10.1016/S0921-4526(96)00817-4
[17]
Blanter M, Golovin I S. Internal Friction. Encyclopedia of iron, steel, and their alloys. New York: Taylor and Francis, 2016
[18]
Blanter M S, Golovin I S, Neuhäuser H, et al. Internal friction in metallic materials. Berlin: Springer, 2007
[19]
Zeger A, Shiller P. Kinks at dislocations and their effect on internal friction in crystals. Physical Acoustics (Russian translation). Moscow: Mir, 1969
[20]
Kaminskii V V, Lyubimova Y V, Romanov A E. Probing of polycrystalline magnesium at ultrasonic frequencies by mechanical spectroscopy. Mater Phys Mechan, 2020, 44, 19 doi: 10.18720/MPM.4412020_3
Fig. 1.  Young's modulus temperature dependencies in polycrystalline SmS at various annealing temperatures: 1: without annealing, 2: 673 K, 3: 913 K, 4: 1073 K. The “step” observed at approximately 135 K in spectra 1 and 2 disappears with an increase in the annealing temperature (see spectrum 4).

Fig. 2.  X-ray diffraction patterns of the sample: 1: initial state (sample surface), 2: after heat treatment (sample cleavage). The reflection peak corresponding to plane (111) disappears after annealing; the reflection intensity peak (200) decreases twice after annealing.

Fig. 3.  Temperature dependencies of the attenuation decrement at different annealing temperatures: 1: without annealing, 2: 673 K, 3: 913 K, 4: 1073 K. Niblett-Wilks and Bordoni peaks are shown as P1 and P2. Annealing of the sample leads to a disappearance of the peaks since the dislocation density decreases.

Table 1.   Young's modulus at room temperature.

CalculationYoung's modulus (GPa)
EV89
ER79, 6
EAVRH84, 31
EGVRH84, 18
Without annealing83, 7
Annealing 673 K83
Annealing 913 K80, 5
Annealing 1073 K78, 9
DownLoad: CSV
[1]
Takenaka K, Asai D, Kaizu R, et al. Giant isotropic negative thermal expansion in Y-doped samarium monosulfides by intra-atomic charge transfer. Sci Rep, 2019, 9, 122 doi: 10.1038/s41598-018-36568-w
[2]
Kaminsky V V, Soloviev S M, Khavrov G D, et al. Mechanism of the semiconductor –metal phase transition in Sm 1 – xGdxS thin films. Semiconductors, 2018, 52(1), 41 doi: 10.1134/S1063782618010116
[3]
Sharenkova N V, Kaminskii V V, Golubkov A V, et al. The structure of a metallic-phase film produced by mechanical polishing of polycrystalline SmS. Phys Solid State, 2005, 47, 622 doi: 10.1134/1.1913970
[4]
Kaminskii V V, Lanyi S. Semiconductor–metal phase transition under a strain induced by a spherical indenter. Tech Phys, 1998, 43, 314 doi: 10.1134/1.1258916
[5]
Sousanis A, Smet P F, Poelman D. Samarium monosulfide (SmS): reviewing properties and applications. Materials, 2017, 10, 953 doi: 10.3390/ma10080953
[6]
Kaminskiĭ V V, Didik V A, Kazanin M M, et al. Thermovoltaic effect in polycrystalline samarium sulfide. Tech Phys Lett, 2009, 35, 981 doi: 10.1134/S1063785009110030
[7]
Kaminskii V V, Solov’ev S M, Khavrov G D, et al. Structural features of Sm1 – xEuxS thin polycrystalline films. Semiconductors, 2017, 51(6), 828 doi: 10.1134/S1063782617060124
[8]
Pronin I A, Averin I A, Bozhinov A S, et al. The thermovoltaic effect in zinc oxide inhomogeneously doped with mixed-valence impurities. Tech Phys Lett, 2015, 41, 930 doi: 10.1134/S1063785015100132
[9]
Kaminsky V V, Molodykh A A, Stepanov N N, et al. The application peculiarities of semi-conducting resistive-strain sensors and baroresistors on the basis of samarium sulphide. Nauchnoe Priborostroenie (Scientific Instrumentation), 2011, 2, 53
[10]
Kustov S, Golyabdin S, Ichino A, et al. A new design of automated piezoelectric composite oscillator technique. Mater Sci Eng A, 2006, 442(1), 532 doi: 10.1016/j.msea.2006.02.230
[11]
Robinson W H, Edgar A. The piezoelectric method of determining mechanical damping at frequencies of 30 to 200 kHz. IEEE Trans Sonics Ultrason, 1974, 21(2), 98 doi: 10.1109/T-SU.1974.29798
[12]
Pal’-Val’ P P, Pal’-Val’ L N. Low-temperature internal friction and nanostructured metal stability. Met Sci Heat Treat, 2012, 54, 234 doi: 10.1007/s11041-012-9488-1
[13]
Lin D, Xu L, Jing H, et al. Effects of annealing on the structure and mechanical properties of FeCoCrNi high-entropy alloy fabricated via selective laser melting. Addit Manufact, 2020, 32, 101058 doi: 10.1016/j.addma.2020.101058
[14]
Wang Z, Baker I. Effects of annealing and thermo-mechanical treatment on the microstructures and mechanical properties of a carbon-doped FeNiMnAl multi-component alloy. Mater Sci Eng A, 2017, 693, 101 doi: 10.1016/j.msea.2017.03.099
[15]
Pal-Val P P, Loginov Yu N, Demakov S L, et al. Unusual Young׳s modulus behavior in ultrafine-grained and microcrystalline copper wires caused by texture changes during processing and annealing. Mater Sci Eng A, 2014, 618, 9 doi: 10.1016/j.msea.2014.08.069
[16]
Scharer U, Wachter P. Brillouin spectroscopy on doped SmS. Physica B, 1997, 721, 230 doi: 10.1016/S0921-4526(96)00817-4
[17]
Blanter M, Golovin I S. Internal Friction. Encyclopedia of iron, steel, and their alloys. New York: Taylor and Francis, 2016
[18]
Blanter M S, Golovin I S, Neuhäuser H, et al. Internal friction in metallic materials. Berlin: Springer, 2007
[19]
Zeger A, Shiller P. Kinks at dislocations and their effect on internal friction in crystals. Physical Acoustics (Russian translation). Moscow: Mir, 1969
[20]
Kaminskii V V, Lyubimova Y V, Romanov A E. Probing of polycrystalline magnesium at ultrasonic frequencies by mechanical spectroscopy. Mater Phys Mechan, 2020, 44, 19 doi: 10.18720/MPM.4412020_3
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    Received: 09 June 2020 Revised: 23 July 2020 Online: Accepted Manuscript: 08 September 2020Uncorrected proof: 11 September 2020Published: 10 March 2021

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      V. V. Kaminskii, N. V. Sharenkova, G. A. Kamenskaya, M. A. Grevtsev, Yu. V. Lyubimova. Anomalies in Young's modulus behavior after annealing in polycrystalline SmS[J]. Journal of Semiconductors, 2021, 42(3): 032101. doi: 10.1088/1674-4926/42/3/032101 V V Kaminskii, N V Sharenkova, G A Kamenskaya, M A Grevtsev, Y V Lyubimova, Anomalies in Young\'s modulus behavior after annealing in polycrystalline SmS[J]. J. Semicond., 2021, 42(3): 032101. doi: 10.1088/1674-4926/42/3/032101.Export: BibTex EndNote
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      V. V. Kaminskii, N. V. Sharenkova, G. A. Kamenskaya, M. A. Grevtsev, Yu. V. Lyubimova. Anomalies in Young's modulus behavior after annealing in polycrystalline SmS[J]. Journal of Semiconductors, 2021, 42(3): 032101. doi: 10.1088/1674-4926/42/3/032101

      V V Kaminskii, N V Sharenkova, G A Kamenskaya, M A Grevtsev, Y V Lyubimova, Anomalies in Young\'s modulus behavior after annealing in polycrystalline SmS[J]. J. Semicond., 2021, 42(3): 032101. doi: 10.1088/1674-4926/42/3/032101.
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      Anomalies in Young's modulus behavior after annealing in polycrystalline SmS

      doi: 10.1088/1674-4926/42/3/032101
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      • Author Bio:

        V. V. Kaminskii is currently a postgraduate student at ITMO University. Graduated from the bachelor's degree at the Peter the Great St. Petersburg Polytechnic University. He received master's degree from ITMO University. His research area includes the study of metallic and semiconducting materials by mechanical and impedance spectroscopy. Of particular interest is its samarium sulfide and sensors based on it

        Yu. V. Lyubimova got her Ph.D. in Physical and Mathematical Sciences in 2018 at ITMO University. Now she works at ITMO University as a researcher. Her research interests are related to the study of the properties and motion of domain walls in ferroics by mechanomagnetic and mechanical spectroscopy. Yu. V Lyubimova actively collaborates with foreign scientific groups in her research area

      • Corresponding author: vvkaminskii@itmo.ru
      • Received Date: 2020-06-09
      • Revised Date: 2020-07-23
      • Published Date: 2021-03-10

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